Development of the first peptide retention prediction model for immobilized artificial membrane phosphatidylcholine (IAM.PC) stationary phase is reported. 2D LC-MS/MS analysis of a whole cell lysate of S. cerevisiae yielded a retention dataset of ~29,500
Daniel Gussakovsky +3 more
doaj +3 more sources
Retention of Anions on Silica-based Metalloporphyrin Stationary Phases
The silica-based Fe(III)-protoporphyrin and Zn-tetraphenylporphyrin stationary phases were examined for the HPLC separation of anions. The retention of nine common inorganic anions as well as benzoate anion (BA) and its hydroxy analogues (HBA) was examined using tartrate, acetate, and succinate eluents.
BIESAGA, Magdalena +3 more
openaire +3 more sources
Electrochromatographic retention of peptides on strong cation‐exchange stationary phases [PDF]
AbstractWe analyze the systematic and substantial electrical field‐dependence of electrochromatographic retention for four counterionic peptides ([Met5]enkephalin, oxytocin, [Arg8]vasopressin, and luteinizing hormone releasing hormone (LHRH) ) on a strong cation‐exchange (SCX) stationary phase.
Ivo, Nischang +2 more
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Normal and reversed phase high performance liquid chromatography of some new 1, 2, 4-triazole derivatives [PDF]
The retention behaviour and separation ability of normal and reversed phase HPLC with one non-polar and two polar mobile phases, have been studied by measuring the retention constants of a series of newly synthesized 1,2,4-triazole derivatives.
Ačanski Marijana M. +2 more
doaj +1 more source
Retention of Halogenated Solutes on Stationary Phases Containing Heavy Atoms [PDF]
To examine the effects of weak intermolecular interactions on solid-phase extraction (SPE) and chromatographic separation, we synthesized some novel stationary phases with a heavy atom effect layer by immobilizing halogenated aromatic rings and hydroxyl groups onto the surface of a hydrophilic base polymer.
Toshio Miwa +3 more
openaire +3 more sources
Separation and lipophilicity of some new steroid derivatives in normal- and reversed-phase high performance liquid chromatography [PDF]
The separation ability and retention of normal and reversed phase HPLC with, respectively, three non-polar and two polar mobile phases, have been studied by measuring the retention constants of a series of newly synthesized estrone derivatives.
Ačanski Marijana M. +2 more
doaj +1 more source
Normal and reversed phase thin-layer chromatography of new 16,17-secoestrone derivatives [PDF]
The retention behaviour and separation ability of a series of new 16,17-secoestrone derivatives has been studied on silica gel, alumina and C-18 silica gel layers with non-aqueous and aqueous-organic mobile phases.
SUZANA JOVANOVIC-SANTA +2 more
doaj +3 more sources
A novel ZIF-8 assisted polyacrylamide functionalized silica polar stationary phase was prepared by a facile method of adding ZIF-8 nanoparticles and silica into polyacrylamide (PAM) aqueous solution, and then stirring the mixture until the solution was ...
Tong Zhang +5 more
doaj +1 more source
There are several different approaches for LC method development; beside traditional, different software programs for method development and optimization are available.
Tina Snoj Ekmečič, Irena Kralj Cigic
doaj +1 more source
The application of the extended thermodynamic approach to describe the effect of counterions, both of chaotropic agents and ionic strength modifiers, on the retention behavior of protonated basic analytes in chaotropic chromatography [PDF]
In this study, the extended thermodynamic approach was used to quantitatively explain the effect of counterions, both of chaotropic agents and ionic strength modifiers, in variable (vI) and constant ionic strength (cI) systems on the retention behavior ...
Gkountanas Kostas +4 more
doaj +1 more source

