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The Journal of Physical Chemistry A, 2015
Cationic rhodium clusters, Rh(n)(+) (n = 4-8), were prepared in the gas phase by the laser ablation of a Rh rod. The Rh(n)(+) clusters were introduced into a reaction gas cell filled with nitric oxide (NO) diluted with He, where they were subjected to collisions with NO and He in a thermal equilibrium at 300 K.
Yuki, Tawaraya +3 more
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Cationic rhodium clusters, Rh(n)(+) (n = 4-8), were prepared in the gas phase by the laser ablation of a Rh rod. The Rh(n)(+) clusters were introduced into a reaction gas cell filled with nitric oxide (NO) diluted with He, where they were subjected to collisions with NO and He in a thermal equilibrium at 300 K.
Yuki, Tawaraya +3 more
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A novel thermal desorption spectroscopy apparatus
Review of Scientific Instruments, 2000We present a new experimental setup designed to perform measurements of thermal desorption spectroscopy of hydrogen released from metallic samples. The distinctive features of the proposed arrangement are a compact reactor and the use of a mass flow meter to measure the flux of gas desorbed from the sample. A complete set of hydrogen desorption spectra
Facundo J. Castro, Gabriel Meyer
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Bulk effects in Thermal Desorption Spectroscopy
The Journal of Chemical Physics, 1998In this work we analyze Thermal Desorption Spectroscopy (TDS) experiments of gases considering simultaneously atomic diffusion in the bulk and recombinative reaction on the surface of a solid sample. We perform computer simulations in a three-dimensional cubic lattice, and compare the simulated spectra with numerical results from a simple reaction ...
Facundo J. Castro +2 more
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On the Methodology of Thermal Desorption Spectroscopy to Evaluate Hydrogen Embrittlement
Materials Science Forum, 2012Thermal desorption spectroscopy (TDS) is a very important tool in hydrogen embrittlement (HE) related research and has been applied on many different materials over the last decades in order to improve knowledge on the HE phenomenon. TDS provides the opportunity to distinguish between different types of hydrogen traps based on the analysis of a ...
Pérez Escobar, D. +3 more
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Thermal Desorption Spectroscopy
2018TDS is a method for the study of adsorption, desorption, and reaction of adsorbed atoms or molecules on surfaces by measuring the desorption rate of desorbing gas from surfaces as a function of sample temperature. The basic concept of this method is that adsorbates with a higher desorption barrier desorb at higher temperature.
Shohei Ogura, Katsuyuki Fukutani
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The study of “microsurfaces” using thermal desorption spectroscopy
Thin Solid Films, 1979The use of a newly combined ultrahigh vacuum technique for studying continuous and particulate evaporated thin films using thermal desorption spectroscopy (TDS), transmission electron microscopy (TEM), and transmission electron diffraction (TED) is discussed. It is shown that (1) CO thermal desorption energies of epitaxially deposited (111) Ni and (111)
M.E. Thomas, H. Poppa, G.M. Pound
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Magic-angle thermal desorption mass spectroscopy
Surface Science, 1990Abstract Accurate quantitative measurements of desorption rates or adsorbate coverages in thermal desorption mass spectroscopy (TDS) using line-of-sight mass spectrometers are hindered by the fact that the angular distributions of desorption flux can vary widely from desorbate to desorbate, ranging from cos1o to cos9 o for most species studied to ...
Steven W. Pauls, Charles T. Campbell
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Field emission thermal desorption spectroscopy
Review of Scientific Instruments, 1982Thermal desorption spectra from single crystal planes of a field emitter are obtained with the technique described. The specimen temperature is varied linearly and the field emission current from the face of interest is recorded vs temperature. Heating current and temperature measurements are transmitted to and from the tip using digital techniques via
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Structural characterization of a-SiC:H by thermal desorption spectroscopy
Applied Surface Science, 1993Abstract The structure of a-Si1−xCx:H thin films prepared from different mixtures of SiH4 and CH4 was studied by thermal desorption spectroscopy. The influence of the gas phase composition and the thickness on the hydrogen evolution spectra is presented and discussed.
F. Maass +6 more
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Thermal desorption spectroscopy of he from Ni at and below saturation
Radiation Effects, 1983Abstract Trapping of helium after implantation at energies of 8 to 150 keV and fluences up to 1019 He-ions/cm2 in nickel at room temperature is studied by measuring the thermal desorption spectra during linear heating up to 1000°C. At several annealing stages the trapped helium is measured by means of the nuclear reaction 3He(d, α)H and the target ...
Ehrenberg, J. +2 more
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