Results 71 to 80 of about 601,668 (305)

Mechanochemical Synthesis and Characterization of Nanostructured ErB4 and NdB4 Rare‐Earth Tetraborides

open access: yesAdvanced Engineering Materials, Volume 27, Issue 6, March 2025.
ErB4 and NdB4 nanostructured powders are produced by mechanochemical synthesis. 5 h mechanical alloying and 4 M HCl acid leaching are used in the production. ErB4 and NdB4 powders exhibit maximum magnetization of 0.4726 emu g−1 accompanied with an antiferromagnetic‐to‐paramagnetic phase transition at about TN = 18 K and 0.132 emu g−1 with a maximum at ...
Burçak Boztemur   +5 more
wiley   +1 more source

Depth Profiling and Internal Structure Determination of Low Dimensional Materials Using X-ray Photoelectron Spectroscopy

open access: yes, 2015
Properties of any heterostructured material depend critically on the specific composition profile of the constituent elements in the sample. X-ray photoelectron spectroscopy (XPS) is particularly well suited to probe elemental composition of any system ...
D. D. Sarma   +5 more
core   +1 more source

ZnO/ZnAl2O4 Nanocomposite Films Studied by X-Ray Diffraction, FTIR, and X-Ray Photoelectron Spectroscopy

open access: yesJournal of Spectroscopy, 2015
ZnO/ZnAl2O4 nanocomposite films were synthesised by ultrasonic spray pyrolysis (USP) by extracting Al2O(SO4)2 oxide with zinc chloride hydrate in deionised water.
S. Iaiche, A. Djelloul
doaj   +1 more source

Low‐Cost, Large‐Scale Nanoporous Metals by Mechanical Alloying, Oxide Reduction, and Dealloying of Powders

open access: yesAdvanced Engineering Materials, EarlyView.
Powder metal processing provides scalable advantages in nanoporous (np) metal development. Mechanical alloying is used to produce unique precursors for hybrid nanopore formation by oxide reduction and dealloying. As demonstrated in np Ag, this approach improves process efficiency while promoting smaller ligaments and larger pores, both of which are ...
Mark A. Atwater, Oliver A. Fowler
wiley   +1 more source

Selenium Valence-to-Core X-ray Emission Spectroscopy and Kβ HERFD X-ray Absorption Spectroscopy as Complementary Probes of Chemical and Electronic Structure

open access: yes, 2021
Selenium X-ray absorption spectroscopy (XAS) has found widespread use in investigations of Se-containing materials, geochemical processes, and biological active sites.
Justin T., Henthorn, Serena, DeBeer
core   +1 more source

Non-uniform interval-pulse X-ray photon correlation spectroscopy for reduced exposure

open access: yesJournal of Synchrotron Radiation
X-ray photon correlation spectroscopy (XPCS) is a powerful technique for evaluating microscopic dynamics using coherent X-rays. Detecting fast or small-scale dynamics typically requires strong illumination and wide-angle scattering detection; however ...
Taiki Hoshino, Jingmin Tang
doaj   +1 more source

SnCl4/nano-sawdust as an Efficient Bio-based Catalyst for the Synthesis of 2-Substituted Benzothiazoles and Benzimidazoles [PDF]

open access: yesJournal of Nanostructures, 2019
SnCl4/nano-sawdust was prepared as a carbohydrate-based catalyst containing of tin bearing cellulose units. The catalyst was characterized by X-ray diffraction (XRD), fourier transform infrared spectroscopy (FT-IR), field emission scanning electron ...
Bi Bi Fatemeh Mirjalili   +3 more
doaj   +1 more source

Electrochemical Evaluation of Compressed Selective Laser Melted AlSi7Mg and AlSi10Mg Alloys in Chloride Environment

open access: yesAdvanced Engineering Materials, EarlyView.
The corrosion performance of AlSi7Mg and AlSi10Mg alloys produced through selective laser melting (SLM) was examined under compressive stress in a chloride environment. Electrochemical analyses, including open‐circuit potential (OCP), potentiodynamic polarization (CPP), and electrochemical impedance spectroscopy (EIS), were complemented by scanning ...
Femi John Akinfolarin   +2 more
wiley   +1 more source

Studying individual magnetic nanoparticles with X-ray PEEM [PDF]

open access: yes, 2014
The thesis addresses a subject with broad implications in various scientific and technical areas. It presents unique direct observations of the magnetic state of single particles of iron (Fe), cobalt (Co) and nickel (Ni) with nanoscopic dimensions by ...
Balan, Ana-Maria
core   +1 more source

X-ray absorption spectroscopy—a beginner’s guide

open access: yesJPhys Energy
X-ray absorption spectroscopy (XAS) has become a central tool for probing the local electronic and atomic structure of materials across physics, chemistry, and materials science, particularly under realistic operating conditions.
Marcus Fehse, Lorenzo Stievano
doaj   +1 more source

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