Results 31 to 40 of about 475,171 (162)

On-Site Measurement of Fat and Protein Contents in Milk Using Mobile NMR Technology

open access: yesMolecules, 2022
Robust and easy-to-use NMR sensor technology is proposed for accurate, on-site determination of fat and protein contents in milk. The two parameters are determined using fast consecutive 1H and 35Cl low-field NMR experiments on milk samples upon the 1:1 ...
Morten K. Sørensen   +4 more
doaj   +1 more source

CASD-NMR: critical assessment of automated structure determination by NMR [PDF]

open access: yes, 2009
NMR spectroscopy is currently the only technique for determining the solution structure of biological macromolecules. This typically requires both the assignment of resonances and a labor-intensive analysis of multidimensional nuclear Overhauser effect ...
NMR Spectroscopy   +4 more
core   +1 more source

Steady-State Free Precession sequences for high and low field NMR spectroscopy in solution: Challenges and opportunities

open access: yesJournal of Magnetic Resonance Open, 2023
The receptivity of NMR spectroscopy is low when compared to other techniques. Historically, increasing the strength of the static magnetic field has been the major approach to increase NMR sensitivity.
Tiago Bueno Moraes   +5 more
doaj   +1 more source

Using 2D experiments with reverse heteronuclear correlation on a benchtop NMR spectrometer X-Pulse to study the structure of gemfibrozil

open access: yesРазработка и регистрация лекарственных средств, 2021
The article discusses application of two powerful NMR techniques ME-HSQC and HMBC to determine the structure of gemfibrozil molecules as an example on the benchtop NMR spectrometer X-Pulse.

doaj  

Nuclear magnetic resonance (NMR) applied to membrane-protein complexes [PDF]

open access: yes, 2016
Increasing evidence suggests that most proteins occur and function in complexes rather than as isolated entities when embedded in cellular membranes.
Baldus, Marc   +5 more
core   +2 more sources

RotoMate: An open-source, 3D printed autosampler for use with benchtop nuclear magnetic resonance spectrometers

open access: yesHardwareX, 2021
Benchtop nuclear magnetic resonance (NMR) spectrometers are versatile analytic instruments with low acquisition and operation cost. However, in the basic version, samples must be manually measured one after the other.
Marco Dyga   +2 more
doaj   +1 more source

[O─I─O]+ Halogen‐Bonded Complexes of Pyridine N‐Oxides

open access: yesAngewandte Chemie, EarlyView.
The missing puzzle of 3‐center‐4‐electron halogen‐bonded complexes viz. [O─I─O]+ of pyridine N‐oxides are structurally characterized by x‐ray diffraction. Monodentate N‐oxide O‐atom acts as the halogen bond acceptor. Their solution complexations are characterized by 15N NMR spectroscopy.
Rakesh Puttreddy   +3 more
wiley   +2 more sources

From Berzelius to Hyperspace: Previously Unrecognized Network of Reactivity in Textbook Brominations

open access: yesAngewandte Chemie, EarlyView.
Robotic scans across multidimensional condition spaces of classic bromination reactions uncover regions of previously unrecognized reactivity, yielding new major products and novel substitution patterns. Correlation and anticorrelation analyses of product distributions across these hyperspaces enable reconstruction of the underlying mechanistic ...
Yankai Jia   +9 more
wiley   +2 more sources

Digitally Based Precision Time-Domain Spectrometer for NMR Relaxation and NMR Cryoporometry

open access: yesMicro, 2023
NMR Relaxation (NMRR) is an extremely useful quantitative technique for material science, particularly for studying polymers and porous materials. NMR Cryoporometry (NMRC) is a powerful technique for the measurement of pore-size distributions and total ...
John Beausire Wyatt Webber, Pavel Demin
doaj   +1 more source

Hyperpolarized 129Xe for benchtop NMR: Inline instrumentation for automated yet flexible operation yielding high polarization

open access: yesJournal of Magnetic Resonance Open
The use of hyperpolarized media in combination with benchtop NMR spectrometers is currently extensively investigated to enable cost effective but highly sensitive applications.
Wolfgang Kilian   +3 more
doaj   +1 more source

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