Objective:This study aimed to develop and validate a method using a high-performance liquid chromatography (HPLC) to perform a quantitative analysis of nebivolol (NEB) and amlodipine (AML) along with some related substances in the synthetic mixture ...
Cem ÖNAL+3 more
doaj +1 more source
Photodegradation Mechanisms of Tetraphenyl Butadiene Coatings for Liquid Argon Detectors [PDF]
We report on studies of degradation mechanisms of tetraphenyl butadiene (TPB) coatings of the type used in neutrino and dark matter liquid argon experiments. Using gas chromatography coupled to mass spectrometry we have detected the ultraviolet-blocking impurity benzophenone (BP).
arxiv +1 more source
Presurgery 72‐h fasting in GB patients leads to adaptations of plasma lipids and polar metabolites. Fasting reduces lysophosphatidylcholines and increases free fatty acids, shifts triglycerides toward long‐chain TGs and increases branched‐chain amino acids, alpha aminobutyric acid, and uric acid.
Iris Divé+7 more
wiley +1 more source
The way to ultrafast, high-throughput enantioseparations of bioactive compounds in liquid and supercritical fluid chromatography [PDF]
Until less than 10 years ago, chiral separations were carried out with columns packed with 5 or 3 μm fully porous particles (FPPs). Times to resolve enantiomeric mixtures were easily larger than 30 min, or so.
Catani, Martina+8 more
core +2 more sources
Cloud point extraction coupled with back extraction: a green methodology in analytical chemistry
Recently, cloud point extraction (CPE) coupled with back extraction (BE) has been suggested as a promising alternative to liquid-liquid extraction. In CPE, non-ionic surfactants in aqueous solutions form micelles and the solution becomes turbid when ...
Shivpoojan Kori
doaj +1 more source
Synthesis of hydrogen- and methyl-capped long-chain polyynes by intense ultrashort laser pulse irradiation of toluene [PDF]
Hydrogen- and methyl-capped polyynes were synthesized by irradiating pure liquid toluene with 35 femtosecond, 300 {\mu}J laser pulses having a central wavelength of 800 nm, generated by a regeneratively amplified Ti:sapphire tabletop laser at a repetition rate of 1 kHz.
arxiv +1 more source
Elevated level of cholesterol is positively correlated to prostate cancer development and disease severity. Cholesterol‐lowering drugs, such as statins, are demonstrated to inhibit prostate cancer. VNPP433‐3β interrupts multiple signaling and metabolic pathways, including cholesterol biosynthesis, AR‐mediated transcription of several oncogenes, mRNA 5′
Retheesh S. Thankan+10 more
wiley +1 more source
Detection strategies for bioassays based on liquid chromatography, fluorescence spectroscopy and mass spectrometry [PDF]
New detection strategies for bioassays based on liquid chromatography,\ud fluorescence spectroscopy and mass spectrometry were developed and are\ud presented within this ...
Hempen, Christel Maria
core +1 more source
New Trends in Fast Liquid Chromatography
Analytical laboratories are currently interested in enhancing overall productivity by increasing sample throughput and reducing analysis time.
Dao T.-T. Nguyen+3 more
doaj +1 more source
Determination of carbohydrates in infant milk powders by ultra-performance liquid chromatography with evaporative light scattering detector and BEH HILIC column [PDF]
The possibility of carbohydrate separation in BEH HILIC (Ethylene Bridged Hybride, Hydrophilic Interaction Liquid Chromatography) column was studied by ultra-performance liquid chromatography (UPLC) with evaporative light scattering detector (ELSD) and mobile phase containing amine compounds as modifiers.
arxiv