Electrospray Ionization Mass Spectrometric Analysis of Highly Reactive Glycosyl Halides
Highly reactive glycosyl chlorides and bromides have been analysed by a routine mass spectrometric method using electrospray ionization and lithium salt adduct-forming agents in anhydrous acetonitrile solution, providing salient lithiated molecular ions [
Lajos Kovács +6 more
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We present a simple and cost-effective method for generating a dielectric barrier discharge (DBD) plasma using a commercially available ozone generator power supply.
Yunshuo Tian +2 more
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Determination of Pharmaceuticals in Coastal Systems Using Solid Phase Extraction (SPE) Followed by Ultra Performance Liquid Chromatography – tandem Mass Spectrometry (UPLC-MS/MS) [PDF]
This paper describes the optimization and validation of an analytical method for the determination of 83 pharmaceutically active compounds (PhACs) in aqueous samples using solid-phase extraction (SPE) followed by ultra performance liquid chromatography ...
Baena Nogueras, Rosa María +3 more
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Mechanistic analysis of an asymmetric palladium-catalyzed conjugate addition of arylboronic acids to β-substituted cyclic enones. [PDF]
An asymmetric palladium-catalyzed conjugate addition reaction of arylboronic acids to enone substrates was investigated mechanistically. Desorption electrospray ionization coupled to mass spectrometry was used to identify intermediates of the catalytic ...
Boeser, Cornelia L +5 more
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High Sensitivity Mass Spectrometric Quantification of Serum Growth Hormone by Amphiphilic Peptide Conjugation [PDF]
Amphiphilic peptide conjugation affords a significant increase in sensitivity with protein quantification by electrospray-ionization mass spectrometry.
Arsene +25 more
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Liquid chromatography tandem mass spectrometry analysis of synthetic coccidiostats in eggs [PDF]
Coccidiostats are synthetic drugs administered to animals, especially to poultry, to cure coccidiosis. In this paper, we present a selective liquid chromatography-tandem mass spectrometry (LC-MS/MS) method to analyze residues of five synthetic ...
Buiarelli, Francesca +6 more
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An overview of the current literature on the chemical processes involved in the ion formation from low molecular weight organic compounds by electrospray ionization mass spectrometry is given.
Crotti Antônio Eduardo Miller +3 more
doaj
Recent trends in analytical methods to determine new psychoactive substances in hair [PDF]
New Psychoactive Substances (NPS) belong to several chemical classes, including phenethylamines, piperazines, synthetic cathinones and synthetic cannabinoids.
García Algar, Oscar +4 more
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Human myocardial protein pattern reveals cardiac diseases [PDF]
Proteomic profiles of myocardial tissue in two different etiologies of heart failure were investigated using high performance liquid chromatography (HPLC)/Fourier transform ion cyclotron resonance mass spectrometry (FT-ICR MS).
Baykut, Doan +5 more
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Ionization Process and Electrospray.
Scientist observed natural phenomena and found the existence of ions more than 100 years ago. When the historical background of electrospray was surveyed from the view point of the ionization technique, the origin started by the awareness of the charged drops in nature. Our earth is positively charged and abounds in the positive ion.
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