Results 21 to 30 of about 9,914 (265)

Copper-Catalyzed One-Pot Synthesis of N-Sulfonyl Amidines from Sulfonyl Hydrazine, Terminal Alkynes and Sulfonyl Azides

open access: yesMolecules, 2021
N-Sulfonyl amidines are developed from a Cu-catalyzed three-component reaction from sulfonyl hydrazines, terminal alkynes and sulfonyl azides in toluene at room temperature.
Yu Zhao   +3 more
doaj   +1 more source

Organic solvent-free synthesis of sulfonyl hydrazides in water

open access: yesTetrahedron Green Chem, 2023
An organic solvent-free synthesis of sulfonyl hydrazides has been achieved in water. The reactions of equimolar amount of sulfonyl chlorides and hydrazines afforded a series of substituted sulfonyl hydrazides at 60 ​°C for 1 ​h in water as a solvent in ...
Shizuki Noda, Shinji Tanimori
doaj   +1 more source

Novel one-pot process for the synthesis of ethyl 2-imino-4-methyl-2,3-dihydrothiazole-5-carboxylates [PDF]

open access: yesJournal of the Serbian Chemical Society, 2015
A facile one-pot two-step process for the synthesis of ethyl 2-imino-4-methyl-2,3-dihydrothiazole-5-carboxylates via the cyclocondensation of ethyl 2-thiocyanatoacetoacetate with a variety of hydrazine and hydrazide derivatives has been ...
Beyzaei Hamid, Aryan Reza, Moghadas Hadi
doaj   +1 more source

ON THE OXIDATION OF HYDRAZINE. II. [PDF]

open access: yesJournal of the American Chemical Society, 1907
n ...
Browne, A. W., Shetterly, F. F.
openaire   +6 more sources

Phthaloylation of amines, hydrazines, and hydrazides by N-substituted phthalimides using recyclable sulfated polyborate

open access: yesResults in Chemistry, 2022
An efficient, fast, and environmentally gentle protocol for phthaloylation of amines, hydrazines and hydrazides via transamidation is described. The current research focuses on the phthaloylation of alicyclic, aliphatic, aromatic, heterocyclic amines ...
Prerna Ganwir   +2 more
doaj   +1 more source

Cyanothioacetamides as a synthetic platform for the synthesis of aminopyrazole derivatives

open access: yesBeilstein Journal of Organic Chemistry, 2023
It was shown that the reaction of 2-cyanothioacetamides with hydrazine involves both cyano- and thioamide groups, and 3,5-diaminopyrazoles are formed. In the reaction of 2-cyano-3-(dimethylamino)-N,N-dimethylprop-2-enethioamides with hydrazine and its ...
Valeriy O. Filimonov   +4 more
doaj   +1 more source

2-tert-Butyl-5,6,7,8,9,10-hexahydrocyclohepta[b]indole

open access: yesMolbank, 2011
2-tert-Butyl-5,6,7,8,9,10-hexahydrocyclohepta[b]indole was synthesized by reaction of cycloheptanone and (4-tert-butylphenyl)hydrazine hydrochloride in the presence of sodium acetate and sulfuric acid in glacial acetic acid via Fischer indole synthesis.
Janina Wobbe   +5 more
doaj   +1 more source

Synthesis of the Fmoc-aza-Arg(Boc)2 precursor via hydrazine alkylation; pp. 438–443 [PDF]

open access: yesProceedings of the Estonian Academy of Sciences, 2014
The aza-arginine precursor Fmoc-aza-Arg(Boc)2 was synthesized starting from mono-protected hydrazines via an aza-ornithine precursor. This reaction path is shorter and more efficient than the reductive alkylation reaction.
Anton Mastitski   +2 more
doaj   +1 more source

Reductive Hydrazination with Trichlorosilane: A Method for the Preparation of 1,1-Disubstituted Hydrazines

open access: yes, 2016
A straightforward and facile method has been developed to prepare 1,1-disubstituted hydrazines via Lewis base promoted direct reductive hydrazination. Under the catalysis of hexamethylphosphoramide (HMPA) and N,N-dimethylacetamide (DMAc), respectively ...
Di, X   +5 more
core   +2 more sources

Ultrasonics Promoted Synthesis of 5-(Pyrazol-4-yl)-4,5-Dihydropyrazoles Derivatives

open access: yesApplied Sciences, 2013
A series of new 1,3-diaryl-5-(1-phenyl-3-methyl-5-chloropyrazol-4-yl)-4,5-dihydropyrazole derivatives have been synthesized under sonication conditions in ethanol or methanol/glacial acetic acid mixture (5/1 ratio) with two equivalents of hydrazines and ...
Manuel Nogueras   +4 more
doaj   +1 more source

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