Results 201 to 210 of about 10,658 (268)

Mechanochemical SNAr on Phthalonitriles: Distinct Reactivity and Selectivity in One‐Pot Synthesis for Greener Phthalocyanines

ChemSusChem, Volume 19, Issue 11, 15 June 2026.
Mechanochemical nucleophilic aromatic substitution enables efficient, reproducible functionalization of phthalonitriles under minimal solvent conditions with high versatility. Integrating this process with solid‐state cyclotetramerization affords metalated and metal‐free phthalocyanines in a streamlined sustainable one‐pot workflow.
Obed Rodriguez‐Perez, Daniel Langerreiter, Sandra Kaabel, Eduardo Anaya‐Plaza   +3 more
wiley   +1 more source

Mechanochemical synthesis of π-conjugated naphthotetrathiophene-based covalent organic frameworks and their post-modification <i>via</i> the Doebner reaction. [PDF]

Chem Sci
Gohari MH, Ghamari P, Hamzehpoor E, Effaty F, Friščić T, Perepichka DF.   +5 more
europepmc   +1 more source

Bayesian Optimization of Solvent‐Free Thermal Amidation via Reactive Extrusion

Chemistry – A European Journal, Volume 32, Issue 22, 9 June 2026.
Thermal amidation between a carboxylic acid and an amine was successfully conducted in an extruder in the absence of solvent, coupling agent, or catalyst, relying on an adapted Bayesian Optimization protocol. Active pharmaceutical ingredient moclobemide was synthesized on a larger scale, achieving excellent yield and low Process Mass Intensity (PMI ...
Matthieu Lavayssiere, Xavier Bantreil, Frédéric Lamaty   +2 more
wiley   +1 more source

Mechanochemical Synthesis of α-halo Alkylboronic Esters. [PDF]

Adv Sci (Weinh)
Zhao Y, Yang Z, Wang X, Kang Q, Wang B, Wu T, Lei H, Ma P, Su W, Wang S, Wu Z, Huang X, Fan C, Wei X.   +13 more
europepmc   +1 more source

Mechanochemical Hydrodeoxygenations

European Journal of Organic Chemistry, Volume 29, Issue 22, 9 June 2026.
A silver‐catalyzed mechanochemical hydrodeoxygenation with triethylsilane as reductant allows to convert ketones to the corresponding methylene derivatives in good yields after a short reaction time. Selected examples show that also alcohols, ethers, and sulfoxides can react. In this work, a mechanochemical hydrodeoxygenation (HDO) was developed. Using
Lena M. Hanek, Carsten Bolm
wiley   +1 more source

Efficient mechanochemical synthesis of new fluorinated Schiff bases: a solvent-free, alternative to conventional method with mercury adsorption properties. [PDF]

BMC Chem
Baig MT, Sayed MT, Aledamat R, Hassan S, AlReyashi A, Sidiq N, Al-Qaradawi SY, Mady MF.   +7 more
europepmc   +1 more source

Mechanochemical Synthesis, Characterization and Reactivity of a Room Temperature Stable Calcium Electride. [PDF]

J Am Chem Soc
Bowles AWJ, Quirk JA, Liu Y, Morritt GH, Freitag M, Whitehead GFS, Woodward AW, Brookfield A, Goodwin CAP, Collison D, Tuna F, McMullin CL, Dawson JA, Lu E, Ortu F.   +14 more
europepmc   +1 more source

Wet Mechanochemical Synthesis of BH₄-Substituted Lithium Argyrodites. [PDF]

Small Methods
Han JH, Shin Y, Lee YJ, Ahn S, Lee YS, Yi KW, Cho YW.   +6 more
europepmc   +1 more source

High-Temperature Mechanochemical Synthesis of Nano-ZrO₂ for Enhanced Densification and Fracture Toughness in B₄C Ceramics. [PDF]

Materials (Basel)
Xu J, Jia J, Li B, Fu D, Wang C, Liu K, Wei S, Han Q.   +7 more
europepmc   +1 more source

Mechanochemical Synthesis of MOF-303 and Its CO₂ Adsorption at Ambient Conditions. [PDF]

Molecules
Głowniak S, Szczęśniak B, Choma J, Jaroniec M.   +3 more
europepmc   +1 more source