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Rapid preparative isolation of erythrocentaurin from Enicostemma littorale by medium-pressure liquid chromatography, its estimation by high-pressure thin-layer chromatography, and its α-amylase inhibitory activity.

Journal of Separation Science, 2015
Erythrocentaurin is a relatively simple natural product present among the members of Gentianaceae. A preparative method for the isolation of erythrocentaurin from the ethyl acetate fraction of Enicostemma littorale using medium‐pressure liquid chromatography has been reported.
N. Hassan   +4 more
semanticscholar   +5 more sources

Preparative purification of peoniflorin and albiflorin from peony rhizome using macroporous resin and medium-pressure liquid chromatography.

Journal of Separation Science, 2012
Peoniflorin (PF) and albiflorin (AF) are two principal components of Paeonia species, which exhibit various biological activities such as improvement of blood circulation and immunoregulating function. To further utilization of waste parts of peony plants, an efficient method for preparative purification of these two ingredients from white peony ...
Rong Wang   +6 more
semanticscholar   +5 more sources

Preparative isolation of antioxidative gallic acid derivatives from Saxifraga tangutica using a class separation method based on medium pressure liquid chromatography and reversed phase liquid chromatography.

Journal of Separation Science, 2021
Saxifraga tangutica is widely used as a medicinal herb to treat hepatic diseases. Here, we developed a class separation method to separate of gallic acid derivatives 1,1-diphenyl-2-picrylhydrazyl inhibitors from the methanol extract of Saxifraga ...
J. Dang   +5 more
semanticscholar   +3 more sources

Preparative isolation of 1, 1-diphenyl-2-picrylhydrazyl inhibitors from Ribes himalense using medium-pressure and two-dimensional reversed-phase/reversed-phase liquid chromatography guided by an online HPLC-1, 1-diphenyl-2-picrylhydrazyl assay.

Journal of Separation Science, 2021
The lack of suitable chromatographic purification methods makes it a challenge to effectively isolate the chemical components of traditional Tibetan medicines.
Chuang Liu   +8 more
semanticscholar   +3 more sources

Combination of normal-phase medium-pressure liquid chromatography and high-performance counter-current chromatography for preparation of ginsenoside-Ro from panax ginseng with high recovery and efficiency

Separation and Purification Technology, 2010
Abstract Ginsenoside-Ro which belongs to the oleanane-type saponins has anti-inflammatory, anti-platelet, anticomplementary and immunomodulatory activities. The present paper described the preparation of ginsenoside-Ro from panax ginseng with high recovery and efficiency by combination of normal-phase medium-pressure liquid chromatography (NP-MPLC ...
Yi-Jun Cheng   +5 more
semanticscholar   +4 more sources

One-step separation and purification of three lignans and one flavonol from Sinopodophyllum emodi by medium-pressure liquid chromatography and high-speed counter-current chromatography.

Phytochemical Analysis, 2013
ABSTRACTIntroductionLignans and flavonols are the primary constituents of Sinopodophyllum emodi and have been used as cathartic, anthelmintic, chemotherapeutic and anti‐hypertensive compounds. Although these compounds have been isolated, there have been no reports on the separation of 4′‐demethyl podophyllotoxin, podophyllotoxin, deoxypodophyllotoxin ...
Ping Wang   +6 more
semanticscholar   +5 more sources

Separation and Purification of Sinigrin and Gluconapin from Defatted Indian Mustard Seed Meals by Macroporous Anion Exchange Resin and Medium Pressure Liquid Chromatography

Separation Science and Technology, 2014
Defatted seed meals, the byproducts of Indian mustard seed oil industry, which are just used as animal feedstock and nitrogen fertilizers, possess various nutrients and phytochemical compounds, such as sinigrin and gluconapin. The present study demonstrated a novel, low-cost, and efficient method for the co-production of sinigrin and gluconapin from ...
Tian-Xin Wang, Hao Liang, Qi-Peng Yuan
semanticscholar   +4 more sources

Targeted isolation of 1,1-diphenyl-2-picrylhydrazyl inhibitors from Saxifraga atrata using medium- and high- pressure liquid chromatography combined with online high performance liquid chromatography-1,1-diphenyl-2- picrylhydrazyl detection.

Journal of Chromatography A, 2020
Traditional Tibetan medicine (TTM) is a valuable source of novel therapeutic lead molecules inspired by natural products (NPs). The health benefits of Saxifraga atrata are well documented in TTM, but reports on its chemical composition are limited, most ...
Yangzom Dawa   +7 more
semanticscholar   +3 more sources

Medium-Pressure Liquid Chromatography Coupled to Electrospray Ionization Mass Spectrometry for Separation and On-Line Characterization of Flavonoids from Asparagus officinalis

Chromatographia, 2009
A novel method for separation and on-line characterization of flavonoids from Asparagus officinalis by medium-pressure liquid chromatography coupled to electrospray ionization multi-stage mass spectrometry (MPLC-ESI-MSn) was successfully established. The hyphenation between MPLC and ESI-MSn was designed to keep the split ratio exactly in the range from
Zhi-Guo Hou   +2 more
semanticscholar   +4 more sources

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