Pinacol–Pinacolone Rearrangement Promoted by Polyphosphoric Acid Trimethylsilyl Ester (PPSE) [PDF]
Masa‐aki Kakimoto+2 more
openalex +1 more source
GC–MS analysis of oxysterols and their formation in cultivated liver cells (HepG2)
Abstract Oxysterols play a key role in many (patho)physiological processes and they are potential biomarkers for oxidative stress in several diseases. Here we developed a rapid gas chromatographic‐mass spectrometry‐based method for the separation and quantification of 11 biologically relevant oxysterols bearing hydroxy, epoxy, and dihydroxy groups ...
Elisabeth Koch+6 more
wiley +1 more source
Gas-liquid chromatography of dialkyl, alkyl acyl, and diacyl derivatives of glycerol
Dialkyl, alkyl acyl, and diacyl glycerols were resolved as trimethylsilyl ethers and as acetates by gas-liquid chromatography on a nonpolar stationary phase (OV-1).
Randall Wood+3 more
doaj
Trimethylsilyl Triflate Induced Reaction of Humulene 6,7-Epoxide. Cyclization to 5-Hydroxy-4,8,11,11-tetramethyltricyclo[6.3.0.02,4]undec-9-ene [PDF]
Haruhisa Shirahama+5 more
openalex +1 more source
Iron‐Catalyzed [2+2+2] Cycloadditions for the Construction of Aromatic and Heteroaromatic Rings
Iron catalysis has witnessed numerous applications during the last decades. This review is focused on the developments of iron complexes for the construction of aromatic and heteroaromatic rings by [2+2+2] cycloadditions. The importance of the design of the iron coordination sphere along with the use of several co‐catalysts is discussed, as well as the
William Parisot+4 more
wiley +1 more source
Identification of Diagnostic Biomarkers for Colorectal Polyps Based on Noninvasive Urinary Metabolite Screening and Construction of a Nomogram. [PDF]
Xie Y+7 more
europepmc +1 more source
An a priori design approach identified tyramine as an ideal co‐former for obtaining new supramolecular adducts with nonsteroidal anti‐inflammatory drugs, speeding up the co‐crystallization process. Three novel adducts and a new polymorphic form were synthesized and thoroughly characterized by solid‐state NMR and single‐crystal XRD.
Chiara Rosso+6 more
wiley +1 more source
Precision Synthesis of Boron‐Doped Graphene Nanoribbons: Recent Progress and Perspectives
In this review, recent progress in the bottom‐up organic synthesis and characterization of boron‐doped graphene nanoribbons through on‐surface or in‐solution chemistry is presented. Moreover, the challenges and perspectives in this research field are also discussed.
Jin‐Jiang Zhang, Ji Ma, Xinliang Feng
wiley +1 more source
Urea enhances the yield and quality of bio-oil produced from corncob through pyrolysis. [PDF]
Bello SI+3 more
europepmc +1 more source