Results 51 to 60 of about 25,467 (256)

The state of palladium and copper on the surface of freshly prepared low temperature carbon monoxide oxidadation catalyst PdCl2-CuCl2/γ-Al2O3

open access: yesТонкие химические технологии, 2010
The EXAFS/XANES, XRD, SEM methods were used for examination of freshly prepared low temperature carbon monoxide oxidation in air catalyst PdCl2-CuCl2/γ-Al2O3 active components states.
D. N. Titov   +7 more
doaj  

Phase Engineering of Nanomaterials (PEN): Evolution, Current Challenges, and Future Opportunities

open access: yesAdvanced Materials, EarlyView.
This review summarizes the synthesis, phase transition, advanced characterization spanning ex situ to in situ and operando techniques, and diverse applications of phase engineering of nanomaterials (PEN). It further outlines key challenges and future opportunities, such as phase stability, architecture control, and artificial intelligence (AI)‐driven ...
Ye Chen   +7 more
wiley   +1 more source

CO2 Activation on Lindqvist-Type Polyoxotantalate: Structural Analysis by In Situ HERFD-XANES

open access: yes
Polyoxotantalates, clusters of tantalum (Ta) oxide, are promising catalysts for CO2 fixation reactions because of their exceptional Lewis basicity facilitating CO2 activation.
Naomi Kawamura (2455354)   +6 more
core   +1 more source

TXM-Pal: a companion software for advanced data processing in spectroscopic X-ray microscopy

open access: yesJournal of Synchrotron Radiation
Transmission X-ray microscopy (TXM) is a powerful and non-destructive tool for interpreting the chemical states of a wide range of materials. It utilizes X-ray absorption near-edge structure (XANES) for the chemically sensitive mapping of specific ...
Sugeun Jo, Sangwoo Kim, Jun Lim
doaj   +1 more source

Defect‐Engineered Microwave‐Responsive Ni@C Composites From Waste PET for Catalytic Plastic Upcycling

open access: yesAdvanced Materials, EarlyView.
A circular upcycling strategy transforms waste poly(ethylene terephthalate) bottles into microwave‐responsive Ni@C catalyst featuring lattice‐distorted nickel cores and defective carbon shells. These strain‐rich heterointerfaces enhance dielectric loss and promote localized microwave hotspots, accelerating peroxymonosulfate activation and polymer‐chain
Xiao Lu   +7 more
wiley   +1 more source

Active Phase of Nickel Electrocatalysts Driving Alkaline Hydrogen Evolution

open access: yesAdvanced Materials, EarlyView.
Using depth‐resolved and operando spectroscopic measurements coupled with electrochemical mass spectrometry, the authors uncover the critical role of sub‐surface oxidised species in increasing the activity and durability of Ni‐based cathodes for hydrogen evolution.
Yifeng Wang   +17 more
wiley   +1 more source

Background sequence prediction for TXM-XANES based on polynomial regression and linear interpolation

open access: yesHe jishu
BackgroundFull-field transmission X-ray microscopy (TXM)–X-ray absorption near-edge structural (XANES) (TXM-XANES) is an imaging method that combines TXM and XANES.
XING Yanjun   +5 more
doaj   +1 more source

Sub‐Nanometer Cobalt on Tungsten Titanium Carbide MXene (W2TiC2Tx): An Electrocatalyst for Highly Efficient and Stable Alkaline Hydrogen Evolution at Industrial‐Scale Current Density

open access: yesAdvanced Materials, EarlyView.
A novel W2TiC2Tx MXene prepared through a MAX‐phase route supports sub‐nanometer Co for highly efficient alkaline hydrogen evolution. Strong Co–W interfacial interactions optimize hydrogen adsorption and catalytic activity, enabling low overpotentials of 63 mV at 10 mA cm−2, small Tafel slope of 44.3 mV dec−1, and exceptional durability at industrially
Xiaopeng Liu   +15 more
wiley   +1 more source

Efficient Hydroxyl Diffusion Triggers Surface Hydronium Enrichment and Bulk Proton Participation to Boost Alkaline Hydrogen‐Evolving Reaction

open access: yesAdvanced Materials, EarlyView.
For the first time, we shed light on the surface‐to‐bulk diffusion, induction, and reaction behaviors of OH−, H+, and H2O species on model oxides for alkaline hydrogen‐evolving reaction (HER). We first demonstrate that bulk OH− diffusion significantly affects the generation of proton sources and the diffusion/reaction behaviors of protons, thus ...
Daqin Guan   +12 more
wiley   +1 more source

Photoluminescent properties of porous silicon nanoparticles: synthesis, characterization, and cellular imaging

open access: yesКонденсированные среды и межфазные границы
Purpose: This study investigates the stability of photoluminescent (PL) properties of microporous silicon nanoparticles (μpSi-NPs) synthesized by electrochemical etching of monocrystalline silicon followed by lyophilization.
Darya A. Nazarovskaia   +5 more
doaj   +1 more source

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