One-pot synthesis of highly emissive dipyridinium dihydrohelicenes [PDF]
Condensation of a pyridyl-2-carbaldehyde derivative with 2-(bromoethyl)amine hydrobromide gave tetracyclic pyrido[1,2-a]pyrido[1′,2′:3,4]imidazo-[2,1-c]-6,7-dihydropyrazinium dications in excellent yields. Crystal structures and NOE data demonstrated the
Adriaenssens +25 more
core +1 more source
Cephalopod‐inspired photonic microparticles with dynamic structural coloration are fabricated via confined self‐assembly of linear block copolymers into ellipsoids containing stacked lamellae. Embedded superparamagnetic nanoparticles enable rapid magnetic alignment, restoring vivid, angle‐dependent color.
Gianluca Mazzotta +8 more
wiley +1 more source
One-pot synthesis of difluoromethyl ketones by a difluorination/fragmentation process [PDF]
Difluoromethyl ketones are an under-studied class of ketones which have great potential as useful building blocks for materials and drug design. Here we report a simple and convenient synthesis of this class of compounds via a one-pot difluorination ...
Black, Conor +2 more
core +1 more source
Nucleation‐Controlled Reconstruction of CuOx for Selective CO2 Electroreduction
The ratio of oxygen vacancies (Ov) and exposed Cu2O (111)/(200) of CuOx precatalyst is modulated by nucleation control of Cu(OH)2 precursor. Low Ov ratio and high ratio of Cu2O (111)/(200) in slow‐nucleated CuOx reconstructs to high‐coordinated oxide‐derived copper (OD‐Cu) during electrochemical CO2 reduction reaction (CO2RR) and exhibits enhanced ...
Ying Ying Ch'ng +14 more
wiley +1 more source
Efficient one-pot synthesis of monodisperse alkyl-terminated colloidal germanium nanocrystals [PDF]
An efficient one-pot method for fabricating alkyl-capped germanium nanocrystals (Ge NCs) is reported. Ge NCs with a size of 3.9 ± 0.5 nm, are formed by co-reduction of germanium tetrachloride in the presence of n-butyltrichlorogermane, producing NCs with
Carolan, Darragh, Doyle, Hugh
core +1 more source
Actuating and Sensing Composites of Liquid Crystal Elastomers and Poly(ionic liquid)s
Ionic conductive, mechanically tough, flexible, and stretchable filaments of a composite material comprising a liquid crystal elastomer and a poly(ionic liquid) are produced through 3D printing, which exhibit large actuation strain under stimulation and electrical resistance variation in response to deformation or environmental condition changes. Their
Zeping Liu +6 more
wiley +1 more source
Strategic methods for the preparation of coumarin fused dihydroquinolines (CFDQ): A concise review
Coumarin-fused dihydroquinolines (CFDQs) are fascinating heterocycles that have become intriguing to medicinal chemists due to their outstanding bioactivity.
Reshmi Bose +6 more
doaj +1 more source
"One Pot" Synthesis of 1,5-Diaza-2,3,6,7-Thetrahydro-4-Methyl-Phenanthrene-4,8-Dione From Corresponding Bis-Beta-Amino Acid [PDF]
The cyclization of b-anilino propionic acids in the presence of polyphosphoric acid (PPA) afforded the 2,3-Dihydroquinoline-4-(1H)-ones in good yields. N,N'-bis(2-carboxyethyl)-4-methyl-1,2-diaminobenzene (7) is cyclized under this condition to produce ...
Abbas Shokravi +1 more
doaj
Convenient One-Pot Synthesis of Allylsilanes from Enolizable Ketones
A convenient one-pot synthesis of allylsilanes from enolizable methyl aryl ketones has been developed. The first step involves nucleophilic addition of the trimethylsilylmethyl group to ketones using the alkylation method developed by Ishihara with ...
Man Lung D. Kwan +2 more
doaj +1 more source
One pot solution synthesis of cyclic oligodeoxyribonucleotides
Several cyclic oligodeoxynucleotides with different base composition and size have been prepared from 5',3'-unprotected linear precursors, using a bifunctional phosphorylating reagent. The final deprotected oligomers have been characterized by 1H- and 31P-NMR. The present procedure is particularly useful for millimolar scale syntheses.
Capobianco +5 more
openaire +3 more sources

