Results 11 to 20 of about 18,349 (284)

Convenient approaches to the synthesis of 6-amino- and 6-oxoimidazo[4,5-b]pyrazolo[3,4-e]pyridines

open access: yesЖурнал органічної та фармацевтичної хімії, 2021
Aim. To develop convenient approaches to the synthesis of 6-amino- and 6-oxoimidazo[4,5-b]pyrazolo[3,4-e]pyridines as promising biologically active scaffolds. Results and discussion.
Georgiy G. Yakovenko, Mikhailo V. Vovk
doaj   +1 more source

5-Chloroisoxazoles: A Versatile Starting Material for the Preparation of Amides, Anhydrides, Esters, and Thioesters of 2H-Azirine-2-carboxylic Acids

open access: yesMolecules, 2022
Amides, anhydrides, esters, and thioesters of 2H-azirine-2-carboxylic acids were prepared by a rapid procedure at room temperature involving FeCl2-catalyzed isomerization of 5-chloroisoxazoles to 2H-azirine-2-carbonyl chlorides, followed by reaction with
Anastasiya V. Agafonova   +2 more
doaj   +1 more source

Effects of solvent and structure on the reactivity of 6-substituted nicotinic acids with diazodiphenylmethane in aprotic solvents [PDF]

open access: yesJournal of the Serbian Chemical Society, 2009
The rate constants for the reactions of diazodiphenylmethane (DDM) with 6-substituted nicotinic acids in aprotic solvents at 30°C were determined. The obtained second order rate constants in aprotic solvents, together with literature data for benzoic and
Drmanić Saša Ž.   +2 more
doaj   +3 more sources

The effects of solvents and structure on the electronic absorption spectra of the isomeric pyridine carboxylic acid N-oxides [PDF]

open access: yesChemical Industry and Chemical Engineering Quarterly, 2013
The ultraviolet absorption spectra of the carboxyl group of three isomeric pyridine carboxylic acids N-oxides (picolinic acid N-oxide, nicotinic acid N-oxide and isonicotinic acid N-oxide) were determined in fourteen solvents in the wavelength range ...
Drmanić Saša Ž.   +4 more
doaj   +1 more source

2-(Carboxymethylsulfanyl)pyridine-3-carboxylic acid monohydrate [PDF]

open access: yesActa Crystallographica Section E Structure Reports Online, 2010
The title compound, C(8)H(7)NO(4)S·H(2)O, was obtained by reaction of 2-mercaptopyridine-3-carboxylic acid with chloro-acetic acid. In the mol-ecular structure, the dihedral angle between the two least-squares planes defined by the pyridine ring and the carb-oxy group is 8.32 (9)°.
Xiao-Juan Wang, Yun-Long Feng
openaire   +3 more sources

A Simple Method for Synthesis of Active Esters of Isonicotinic and Picolinic Acids

open access: yesMolecules, 2001
A method for preparation of the p-nitrophenyl-, N-hydroxysuccinimidyl- and pentafluorophenyl esters of isonicotinic and picolinic acids from the corresponding acids is reported.
Jørn B. Christensen
doaj   +1 more source

Rapid and Simultaneous Determination of Free Aromatic Carboxylic Acids and Phenols in Commercial Juices by GC-MS after Ethyl Chloroformate Derivatization

open access: yesSeparations, 2021
Natural phenol and phenolic acids are widely distributed in the plant kingdom and the major dietary sources include fruits and beverages derived therefrom.
Alessio Incocciati   +4 more
doaj   +1 more source

Recurrence of Carboxylic Acid−Pyridine Supramolecular Synthon in the Crystal Structures of Some Pyrazinecarboxylic Acids [PDF]

open access: yes, 2016
X-ray crystal structures of pyrazinic acid 1 and isomeric methylpyrazine carboxylic acids 2−4 are analyzed to examine the occurrence of carboxylic acid−pyridine supramolecular synthon V in these heterocyclic acids. Synthon V, assembled by (carboxyl)O−H···
Ashwini Nangia (1400761)   +2 more
core   +1 more source

Reaction of Pyridine Bases with Carboxylic Acids in Benzene [PDF]

open access: yesBulletin of the Chemical Society of Japan, 1977
Abstract The reaction of pyridine bases with aliphatic monocarboxylic acids has been studied by means of the partition method. Partition was carried out at 25 °C between benzene and 0.10 mol dm−3 (Na, H) ClO4 aqueous solution, the total concentration of pyridine base and that of carboxylic acid being less than 2×10−2 mol dm−3 and 1.0 mol
Katsumi Hirose, Motoharu Tanaka
openaire   +1 more source

Vanadium. Part IX. Oxo-Vanadium (IV) Complexes of Pyridine Carboxylic Acids [PDF]

open access: yes, 1967
The paper describes a number of Oxo-vanadium (IV) complexes of pyridine mono-, di- and tri-carboxylic acids. Pyridine 2-carboxylic acid produces (I) [VO (H2O) (Pic)2 blue, (2) [VO(X) (Pic)2] (where X=pyridine, aniline, α-picoline etc), green and (3) [VO ...
S. Ghosh, R. L. Dutta
core   +1 more source

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