Results 121 to 130 of about 67,105 (299)

Recrystallization (Organic Chemistry Lecture-Demonstrations)

open access: yes, 2021
This lecture-demonstration discusses the principles of recrystallization technique and shows purification of benzoic acid by a single-solvent recrystallization, including removal of insoluble impurities by hot ...
PhD Student Glenn Oldham and Dr Yulia Alekseeva
core  

Bidirectional Photoswitching of a Tailored Azobenzene with Red and Far‐Red Light Involving Triplet Sensitization in an Aqueous System

open access: yesAdvanced Science, EarlyView.
The action spectrum of a tailored azobenzene is shifted toward bio‐optical window through the chemical modification of its singlet and triplet energy levels. Consequently, the bidirectional photo‐switching of azobenzene in physiological conditions is achieved when excited by red and far‐red light, which offers greater tissue penetration.
Mila Miroshnichenko   +11 more
wiley   +1 more source

Autonomous and Continuous Atmospheric Water Harvesting Using Modified Wood

open access: yesAdvanced Science, EarlyView.
A rigid, hydroxyl‐rich wood skeleton with graded channels is used as a multifunctional host to co‐incorporate a PNipam/PAA network and LiCl, creating a high‐performance sorbent for atmospheric water harvesting. The composite achieves rapid sorption, efficient low‐temperature desorption, and stable cycling, enabling a solar‐powered device with a high ...
Shiheng He   +7 more
wiley   +1 more source

Approaches to Modeling of Recrystallization

open access: yes, 2011
Control of the material microstructure in terms of the grain size is a key component in tailoring material properties of metals and alloys and in creating functionally graded materials.
Håkan Hallberg, Hallberg, Håkan
core   +1 more source

Interfacial Polysulfide Confinement via Spatially Controlled Sulfonated Metal–Organic Polyhedra Coatings in Lithium–Sulfur Batteries

open access: yesAdvanced Science, EarlyView.
Spatially controlled sulfonated metal–organic polyhedra (SMOP) coating on sulfur‐loaded hollow carbon spheres form ultrathin, conformal interfacial barriers that selectively confine soluble polysulfides, stabilize sulfur redox, and suppress shuttle reactions.
Soyeon Ko   +8 more
wiley   +1 more source

Effects of Annealing Temperature on Microstructural Evolution and Mechanical Properties in Cold-Rolled High-Nitrogen Austenitic Steel

open access: yesMetals
High-nitrogen austenitic steel (HNS) cold-rolled with a reduction rate of 25% was subjected to an investigation of the effect of annealing temperature on microstructural evolution, tensile properties and the variation in fracture surface morphology.
Jong-Ho Shin   +2 more
doaj   +1 more source

Hybrid CuTCNQ/AgTCNQ metal-organic charge transfer complexes via galvanic replacement vs corrosion-recrystallization

open access: yes, 2014
This study reports a hybrid of two metal-organic semiconductors that are based on organic charge transfer complexes of 7,7,8,8-tetracyanoquinodimethane (TCNQ). It is shown that the spontaneous reaction between semiconducting microrods of CuTCNQ with Ag +
A O'Mullane (20008977)   +3 more
core  

Precipitation‐Modulated Harmonic Architectures Enable Superior Strength–Ductility Synergy from Cryogenic to Elevated Temperatures in Nanostructured Alloys

open access: yesAdvanced Science, EarlyView.
Precipitation‐modulated recrystallization enables a programmable bimodal harmonic architecture in a high‐entropy alloy, delivering 1–2 GPa yield strength with >10% ductility from −196 °C to 700 °C. The resulting broad‐temperature robustness arises from the synergy of dual‐mode nanoprecipitation, harmonic core–shell topology, and temperature‐adaptive ...
Wei Li   +5 more
wiley   +1 more source

Modelling microstructure evolution during equal channel angular pressing of magnesium alloys using cellular automata finite element method

open access: yes, 2013
Equal channel angular pressing (ECAP) is one of the most popular methods of obtaining ultrafine grained (UFG) metals. However, only relatively short billets can be processed by ECAP due to force limitation.
Rosochowski, Andrzej   +3 more
core  

Electric‐Current‐Induced Phase Transformation in Cu6Sn5 Below Its Equilibrium Transition Temperature

open access: yesAdvanced Science, EarlyView.
Electric current induces a monoclinic‐to‐hexagonal phase transformation in Cu6Sn5 at a measured bulk temperature of ∼120°C, below the equilibrium transition temperature. Ex situ synchrotron x‐ray diffraction, TEM, and matched thermal controls show that current stressing promotes the formation of a retained hexagonal η‐phase post‐stress state not ...
Shih‐kang Lin   +3 more
wiley   +1 more source

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