Results 141 to 150 of about 449,097 (372)

Time-Resolved Serial Femtosecond Crystallography at the European XFEL

open access: yesNature Methods, 2019
The European XFEL (EuXFEL) is a 3.4-km long X-ray source, which produces femtosecond, ultrabrilliant and spatially coherent X-ray pulses at megahertz (MHz) repetition rates.
S. Pandey   +47 more
semanticscholar   +1 more source

Synthesis of Bimetallic (Iron–Cobalt) Single Atom Catalysts for Electrochemical Detection of Nitrites

open access: yesAdvanced Materials Technologies, EarlyView.
A CO2 laser‐assisted solid‐state synthesis of a bimetallic single‐atom catalyst is presented. The resulting material consists of a 3D porous graphene support with iron and cobalt atoms anchored as single atoms. Through electrochemical methods, the material's efficiency is demonstrated in the sensitive and selective determination of nitrite, mimicking ...
Guillermo Tostado‐Blazquez   +5 more
wiley   +1 more source

Quasi-Periodic Crystals—The Long Road from Discovery to Acceptance

open access: yesRambam Maimonides Medical Journal, 2013
[Extract] Three surprising discoveries on the nature of matter and its properties were published in the mid-1980s. All these discoveries led to Nobel prizes. The first discovery was in 1985, when fullerenes were discovered by Robert F.
Daniel Schechtman
doaj   +1 more source

Enzyme intermediates captured “on the fly” by mix-and-inject serial crystallography

open access: yesBMC Biology, 2018
Ever since the first atomic structure of an enzyme was solved, the discovery of the mechanism and dynamics of reactions catalyzed by biomolecules has been the key goal for the understanding of the molecular processes that drive life on earth.
J. L. Olmos   +49 more
semanticscholar   +1 more source

Modulating D33 Coefficients Through In Situ AgF and Ag2O Growth in PVDF Composites for High‐Performance Piezoelectric Nanogenerators

open access: yesAdvanced Materials Technologies, EarlyView.
In situ, nanoparticle doping enhances the piezoelectric coefficient (**d₃₃**) of PVDF to ≈12 pC/N, while in situ growth of AgF and Ag₂O dopants increases β‐phase concentration. The nanogenerator achieves a 35 V open‐circuit voltage and 1.6 µA short‐circuit current, powering 10 blue LEDs and charging a 50 nF capacitor within 10 s.
Renjun Liu   +15 more
wiley   +1 more source

Synthesis, Crystal Structures, and Magnetic Properties of Lanthanide (III) Amino-Phosphonate Complexes

open access: yesMagnetochemistry, 2018
Two isostructural lanthanide amino-phosphonate complexes [Ln10(μ3-OH)3(µ-OH)(CO3)2(O2CtBu)15(O3PC6H10NH2)3(O3PC6H10NH3)2(H2O)2][Et2NH2] (Ln = Gd(III), 1 and Tb(III), 2) have been obtained through reflux reactions of lanthanide pivalates with, a ...
Karzan H. Zangana
doaj   +1 more source

Processing serial crystallography data with CrystFEL: a step-by-step guide

open access: yesActa Crystallographica Section D: Structural Biology, 2019
A step-by-step guide to processing serial crystallography data from X-ray free-electron lasers and synchrotron sources using CrystFEL is provided.
T. White
semanticscholar   +1 more source

Chemical Substitution‐Driven Design of a High‐Performance Noncentrosymmetric Bismuth Molybdenum Selenite

open access: yesAdvanced Optical Materials, EarlyView.
The first bismuth molybdenum selenite material with a macroscopic noncentrosymmetric structure is designed using a chemical substitution‐oriented approach and successfully synthesized via a hydrothermal reaction. It exhibits exceptionally well‐balanced nonlinear optical properties, including a s efficiency that is 1.2 times that of KTiOPO4, a suitable ...
Hieu Minh Ngo   +6 more
wiley   +1 more source

Benchmark problems for phase retrieval [PDF]

open access: yesarXiv, 2017
In recent years, the mathematical and algorithmic aspects of the phase retrieval problem have received considerable attention. Many papers in this area mention crystallography as a principal application. In crystallography, the signal to be recovered is periodic and comprised of atomic distributions arranged homogeneously in the unit cell of the ...
arxiv  

Heterogeneously Catalyzed Cascade Oxidative Coupling/Dearomative Spirocyclization of Diarylamines: Facile Access to Spiroacridines

open access: yesAdvanced Synthesis &Catalysis, EarlyView.
Abstract Spirocyclic compounds, particularly spirocyclohexadienones, are important in pharmaceuticals due to their biological activity. In this study, we develop a catalytic cascade oxidative spirocyclization of diarylamines for the rapid access to highly functionalized spirocyclohexadienones. Using commercially available recyclable heterogeneous metal
Kenji Matsumoto   +7 more
wiley   +1 more source

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