Mechanochemical Synthesis of Resveratrol-Piperazine Cocrystals. [PDF]
The 1:1 resveratrol–piperazine cocrystal was successfully synthesized and scaled-up to 300 g scale with the mechanochemical method, as a result of investigating key process parameters, namely the solvent and the grinding time. The use of water, ethanol or ethanol–water mixtures and reaction times up to 50 min were evaluated relative to the dry grinding
Mitran RA +10 more
europepmc +3 more sources
Extending mechanochemical porphyrin synthesis to bulkier aromatics: tetramesitylporphyrin
Aldehydes with bulky substituents in the ortho-positions have been historically difficult in porphyrin synthesis, presumably owing to steric hindrance around the reactive site.
Qiwen Su, Tamara D. Hamilton
doaj +1 more source
Preparation of powder coatings on the surface of steel balls by mechanochemical synthesis
This work presents the results of the study of tribological and corrosion properties of powder coatings based on VN, TiN, SiC and Cr2N obtained by mechanochemical synthesis on the surface of steel balls ShKh15.
Б.К. Рахадилов +4 more
doaj +1 more source
Stochastic kinetics of ribosomes: single motor properties and collective behavior [PDF]
Synthesis of protein molecules in a cell are carried out by ribosomes. A ribosome can be regarded as a molecular motor which utilizes the input chemical energy to move on a messenger RNA (mRNA) track that also serves as a template for the polymerization ...
A. S. Spirin +11 more
core +2 more sources
The effects of mechanochemical synthesis and postsynthetic grinding on the spin crossover material [Fe(atrz)3](BF4)2 was examined in detail using a combination of X-ray diffraction, magnetometry, EXAFS and TEM.
Jed H. Askew +4 more
doaj +1 more source
Mechanochemical activation of batch during fabrication of highly-porous cordierite materials based on natural oxide compounds [PDF]
Using X-ray diffraction analysis and infrared spectroscopy techniques, the effect of additives on phase composition variation during mechanochemical activation of a kaolin-containing cordierite batch was investigated.
Antsiferov V.N. +2 more
doaj +1 more source
Mechanistic Insights into a Sustainable Mechanochemical Synthesis of Ettringite
Mechanochemistry offers an environmentally benign and facile synthesis method for a variety of cement paste constituents. In addition, these methods can be used to selectively tune the properties of cement components.
Dr. Julia Stroh +4 more
doaj +1 more source
TG, FT-IR and NMR characterization of n-C16H34 contaminated alumina and silica after mechanochemical treatment [PDF]
This paper deals with the application of mechanochemistry to model systems composed of alumina or silica artificially contaminated with n-C16H34. The mechanochemical treatment was carried out by means of a ring mill for times ranging from 10 to 40 h ...
L. DE STEFANO +6 more
core +1 more source
Fast synthesis of the polycrystalline materials on the base of Zn 3 V2 MoO11 and Zn 2.5 VMoO8 [PDF]
In our study we applied two different techniques for the preparation of Zn3V2MoO11 and Zn2.5VMoO8 polycrystalline materials - melt quenching method (up-bottom) and mechanochemical synthesis (bottom- up).
Maya Markova-Velichkova, Reni Iordanova
doaj
Mechanochemistry vs Conventional Solid-State Synthesis: A Sustainable Development Pathway [PDF]
The shift to sustainable chemical manufacturing highlights the need for solid-state synthesis methods that minimize solvent use, energy consumption and environmental impact.
Chen Yinuo
doaj +1 more source

