Results 41 to 50 of about 1,824 (162)

A facile microwave assisted one-pot synthesis of novel 1-methylhexahydroquinazolin-5(6H)-ones and bis-1-methylhexahydroquinazolin-5(6H)-ones

open access: yesOrbital: The Electronic Journal of Chemistry, 2011
Novel hexahydroquinazolin-5(6H)-ones 3a-j have been synthesized in good yields by the reaction of enaminones 2a-b with primary amines and formaldehyde under the influence microwaves.
Madhusudhan Saha   +3 more
doaj   +1 more source

Regioselectivity in the multicomponent reaction of 5-aminopyrazoles, cyclic 1,3-diketones and dimethylformamide dimethylacetal under controlled microwave heating

open access: yesBeilstein Journal of Organic Chemistry, 2012
The multicomponent reaction of 5-aminopyrazole derivatives with cyclic 1,3-dicarbonyl compounds and dimethylformamide dimethylacetal (DMFDMA) in DMF at 150 °C under controlled microwave heating afforded regioselectively 8,9-dihydropyrazolo[1,5-a ...
Kamal Usef Sadek   +4 more
doaj   +1 more source

Alum promoted synthesis of 2H-indazolo[2,1-b]phthalazinetrione derivatives in water

open access: yesOrbital: The Electronic Journal of Chemistry, 2012
A new and efficient synthesis of 2H-indazolo[2,1-b]phthalazine-1,6,11(13H)-trione derivatives from the three-component condensation reaction of phthalhydrazide, dimedone, and aromatic aldehydes using alum [KAl(SO4)2.12H2O] as catalyst was ...
Balaji Rajendra Madje   +3 more
doaj   +1 more source

Synthesis of Cyano-Benzylidene Xanthene Synthons Using a Diprotic Brønsted Acid Catalyst, and Their Application as Efficient Inhibitors of Aluminum Corrosion in Alkaline Solutions

open access: yesMolecules, 2022
Novel cyano-benzylidene xanthene derivatives were synthesized using one-pot and condensation reactions. A diprotic Brønsted acid (i.e., oxalic acid) was used as an effective catalyst for the promotion of the synthesis process of the new starting xanthene–
Mohammed A. Amin   +11 more
doaj   +1 more source

Facile and Efficient Synthesis of Xanthene Derivatives Mediated by Lanthanum(III) Nitrate Hexahydrate under Solvent Free Conditions

open access: yesChemistry Journal of Moldova: General, Industrial and Ecological Chemistry, 2020
The present paper shows that lanthanum(III) nitrate hexahydrate can be used as mild and environment friendly homogeneous catalyst for an efficient one-pot multi-component synthesis of biologically active 1,8-dioxo-octahydroxanthene and 14H-dibenzo[a,j ...
Kabeer Ahmed Shaikh   +1 more
doaj   +1 more source

4a′-Hydroxy-3′,3′,5,6′,6′,7-hexamethyl-3′,4′,4a′,6′,7′,9a′-hexahydrospiro[indole-3,9′-xanthene]-1′,2,8′(1H,2′H,5′H)-trione

open access: yesMolbank, 2023
Pseudo-multicomponent reactions (Pseudo-MCRs) have led to a variety of compounds with interesting biological properties, especially desirable in the pharmaceutical industry.
Yuliya E. Ryzhkova   +4 more
doaj   +1 more source

Rh(III)-catalyzed chelation-assisted C–H activation/annulation of 2-arylimidazolines with cyclic diazo-1,3-dicarbonyl compounds: a novel approach to tetracyclic annulated derivatives of 2,3-dihydroimidazo[2,1-a]isoquinoline

open access: yesBeilstein Journal of Organic Chemistry
2-Arylimidazolines were annulated with cyclic diazo-1,3-dicarbonyl compounds under Rh(III)-catalysis for the first time. The developed general and efficient approach based on CH-activation allowed the efficient preparation of five novel types of ...
Ivan Lyutin   +3 more
doaj   +1 more source

Development of a Green Method for the Synthesis of Xanthene-1,8-dione Derivatives from Dimedone and Aldehydes

open access: yesEngineering Proceedings
A green and efficient method was developed for the synthesis of 1,8-dioxo-octahydroxanthene derivatives using linear alkylbenzene sulfonic acid (LABSA) as an eco-friendly Brønsted acid catalyst under aqueous reflux conditions.
Imene Maallem, Malika Berredjem
doaj   +1 more source

Synthesis of Heterocyclic Compounds Derived From Dimedone and Their Anti-tumor and Tyrosine Kinase Inhibitions

open access: yesActa Chimica Slovenica, 2020
The reaction of dimedone with arylaldehydes gave the benzylidene derivatives 3a–c, the latter underwent a series of heterocyclization reactions to give fused thiophene, pyrazole isoxazole and pyridazine derivatives.
Rafat Mohareb   +2 more
doaj   +1 more source

NaHSO4–SiO2 Promoted Solvent-Free Synthesis of Triazolo [1,2-a]indazole-triones [PDF]

open access: yesInternational Journal of New Chemistry, 2014
A new one-pot, efficient three-component condensation of dimedone, urazole and aromatic aldehydes in the presence of silica supported sodium hydrogen sulfate as an effective heterogeneous catalyst for the synthesis of novel Triazolo[1,2-a]indazole-1,3,8 ...
Hossein Anaraki-Ardakani
doaj   +1 more source

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