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Mechanochemical Synthesis of Fluorinated Imines [PDF]
Molecules, 2022 A number of imines, including 12 new compounds, previously not reported in the literature, derived from variously fluorinated benzaldehydes and different anilines or chiral benzylamines were synthesized by a solvent-free mechanochemical method, which was
Karolina Ciesielska +3 more
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Mechanochemical Synthesis of Molecular Chemoreceptors [PDF]
ACS OmegaThe design of environmentally friendly methods for synthesizing molecular receptors is an expanding area within applied organic chemistry. This work systematically summarizes advances in the mechanochemical synthesis of molecular chemoreceptors. It discusses key achievements related to the synthesis of chemoreceptors containing azine, Schiff base ...
Jakub S. Cyniak, Artur Kasprzak
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Mechanochemical Synthesis of Resveratrol–Piperazine Cocrystals [PDF]
MaterialsThe 1:1 resveratrol–piperazine cocrystal was successfully synthesized and scaled-up to 300 g scale with the mechanochemical method, as a result of investigating key process parameters, namely the solvent and the grinding time. The use of water, ethanol or ethanol–water mixtures and reaction times up to 50 min were evaluated relative to the dry grinding
Raúl - Augustin Mitran +2 more
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The mechanochemical synthesis of polymers.
Chem Soc Rev, 2022 Mechanochemistry enables solvent-free syntheses of even novel polymer structures without the need of monomer solubility.
Krusenbaum A +4 more
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Mechanochemical synthesis of organoselenium compounds. [PDF]
Nat CommunAbstractWe disclose herein a strategy for the rapid synthesis of versatile organoselenium compounds under mild conditions. In this work, magnesium-based selenium nucleophiles are formed in situ from easily available organic halides, magnesium metal, and elemental selenium via mechanical stimulation.
Chen S +10 more
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Mechanochemical synthesis of fluoride-ion conducting glass and glass–ceramic in ZrF4–BaF2 binary system [PDF]
Scientific ReportsFluoride glasses in the binary system ZrF4–BaF2 were prepared via mechanochemical treatment. The glass-forming region of the ZrF4–BaF2 system obtained using the mechanochemical method was wider than that obtained using the conventional melt-quenching ...
Kota Motohashi +5 more
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Mechanochemical Synthesis of Nanoparticles for Potential Antimicrobial Applications [PDF]
Materials, 2023 Mietek Jaroniec +2 more
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Mechanochemically Assisted Synthesis of Hexaazatriphenylenehexacarbonitrile [PDF]
The Journal of Organic Chemistry, 2021 1,4,5,8,9,11-hexaazatriphenylenehexacarbonitrile (HAT CN) was synthesized mechanochemically at room temperature. The coupling of hexaketocyclohexane and diaminomaleonitrile was conducted in 10 min by vibratory ball milling. The effects of milling parameters, acids, dehydrating agents, and liquid-assisted grinding were rationalized.
Pickhardt, Wilm +3 more
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Mechanochemically‐Assisted Synthesis of Polyimides [PDF]
ChemSusChem, 2021 AbstractPolyimides were obtained in 99 % yield in under 1 h through the “beat and heat” approach, involving solvent‐free vibrational ball milling and a thermal treatment step. The influence of a plethora of additives was explored, such as Lewis acids, Lewis bases, and dehydrating agents, and the mechanochemical reaction was identified to run via a ...
Tilo Rensch +3 more
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Mechanochemistry in Portugal—A Step towards Sustainable Chemical Synthesis
Molecules, 2021 In Portugal, publications with mechanochemical methods date back to 2009, with the report on mechanochemical strategies for the synthesis of metallopharmaceuticals. Since then, mechanochemical applications have grown in Portugal, spanning several fields,
Vânia André +3 more
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