Polysaccharides, oligosaccharides, and their derivatives, particularly of amylose, cellulose, chitosan, and β-cyclodextrin, are well-known chiral selectors (CSs) of chiral stationary phases (CSPs) in chromatography, because they can separate a wide range
Cuong Viet Bui +2 more
doaj +1 more source
State-of-the-art and recent developments of immobilized polysaccharide-based chiral stationary phases for enantioseparations by high-performance liquid chromatography (2013–2017) [PDF]
Polysaccharide-based chiral stationary phases have been recognized as one of the most powerful ones for high performance liquid chromatography (HPLC) separations of chiral compounds in analytical and also in preparative scale.
Keunchkarian, Sonia, Padró, Juan Manuel
core +4 more sources
Chiral separation of helical chromenes with chloromethyl phenylcarbamate polysaccharide‐based stationary phases [PDF]
AbstractTwo chloromethyl phenylcarbamate‐based chiral stationary phases, one containing an amylose‐type chiral selector (Lux Amylose 2, from Phenomenex) and the other a cellulose‐type one (Lux Cellulose‐4, from Phenomenex), were successfully used for the chiral resolution of three helical chromenes featuring a helicene‐like structure.
Ianni, Federica +7 more
openaire +4 more sources
A novel, validated, reversed-phase (RP), chiral high performance liquid chromatography (HPLC) method was developed for the enantiopurity control analysis of naproxen, a frequently used non-steroidal anti-inflammatory agent using polysaccharide-type ...
Lajos-Attila Papp +5 more
doaj +1 more source
Photografted methacrylate-based monolithic columns coated with cellulose tris(3,5-dimethylphenylcarbamate) for chiral separation in CEC [PDF]
A chiral capillary monolithic column for enantiomer separation in capillary electrochromatography was prepared by coating cellulose tris(3,5-dimethylphenylcarbamate) on porous glycidyl methacrylate-co-ethylene dimethacrylate monolith in capillary format ...
Al-Othman +42 more
core +1 more source
Chromatographic separation of several sets of aromatic position isomers on three cellulose- and one amylose-based chiral stationary phases was performed to evaluate the potential of a polysaccharide-based chiral stationary phase (CSP) in the separation ...
Tohru Shibata +3 more
doaj +1 more source
An Interesting Class of Porous Polymer-Revisiting the Structure of Mesoporous α-d-Polysaccharide Gels [PDF]
The processes involved in the transformation of non-porous, native polysaccharides to their highly porous equivalents introduce significant molecular complexity and are not yet fully understood.
Atichokudomchai +82 more
core +1 more source
Enantioseparation on Riboflavin Derivatives Chemically Bonded to Silica Gel as Chiral Stationary Phases for HPLC [PDF]
International audienceAcetylated and/or 3,5-dimethylphenylcarbamated riboflavins were prepared and the resulting riboflavin derivatives as well as natural riboflavin were regioselectively immobilized on silica gel through chemical bonding at the 5’-O- or
Anger +34 more
core +3 more sources
In this work the separation of the chiral anesthetic compounds ketamine and bupivacaine was development using two chiral stationary phases (CSP).
Ivanildo José da Silva Jr. +2 more
doaj +1 more source
The way to ultrafast, high-throughput enantioseparations of bioactive compounds in liquid and supercritical fluid chromatography [PDF]
Until less than 10 years ago, chiral separations were carried out with columns packed with 5 or 3 μm fully porous particles (FPPs). Times to resolve enantiomeric mixtures were easily larger than 30 min, or so.
Catani, Martina +8 more
core +2 more sources

