Results 111 to 120 of about 15,919 (247)

Novel tetronamides derived from mucobromic acid: synthesis, structural elucidation, DFT calculations and phytotoxic activity

Pest Management Science, EarlyView.
The acyclic mucobromic acid, activated by (1S)‐(+)‐10‐camphorsulfonic acid, afforded the chiral compound 1b, precursor for aza‐Michael addition/elimination on the butenolide yielding tetronamides 2b‐7b. Their relative SRSR configuration was confirmed by the spectrometric methods, DFT calculation and statistical methods.
Kamylla CF Faria, Vitor C Baia, Elson S Alvarenga   +2 more
wiley   +1 more source

Using MALDI‐FTICR Mass Spectrometry to Enhance ZooMS Identifications of Pleistocene Bone Fragments Showing Variable Collagen Preservation

Rapid Communications in Mass Spectrometry, EarlyView.
ABSTRACT Rationale Recent advances in high‐throughput molecular analyses of collagen peptides, especially ZooMS (Zooarchaeology by Mass Spectrometry), have permitted breakthroughs in the analysis of archaeological material that is highly fragmented, a factor that hinders morphological identification.
Pauline Raymond, Karen Ruebens, Fabrice Bray, Jean‐Christophe Castel, Eugène Morin, Foni Le Brun‐Ricalens, Jean‐Guillaume Bordes, Christian Rolando, Jean‐Jacques Hublin   +8 more
wiley   +1 more source

A Method for Identifying Rainfall‐Runoff Events at Sub‐Hourly Time Scales: Applications for Nature‐Based Solutions and Water Resources

River Research and Applications, EarlyView.
ABSTRACT Understanding how changes in catchment conditions affect ecohydrology in response to rainfall‐runoff events is crucial when developing informed strategies to enhance flow resilience, restore natural habitats, interpret water quality data or reduce flood risk.
Josie Ashe, Daniella Montali‐Ashworth, Alan Puttock, Naomi Gatis, David Luscombe, Kirsty Frith, Pia Benaud, Richard E. Brazier   +7 more
wiley   +1 more source

Thermosensitive Nanostructured Coacervates Developed by Mixing ABA‐ and AB‐Block Copolymers and Their Unique Sustained Release of Nano‐Micelles in a Regulated Manner

Small, EarlyView.
Polyion complex micelles composed of blends of ABA and AB block copolymers can form coacervates with a hexagonally packed cylinder nanostructure after heating. The resulting coacervates can release the micelles under physiological conditions in a zero‐order kinetics, possessing cargo proteins.
Takumi Egashira, Hiroshi Kamizawa, Yujiro Hamada, Wataru Fushimoto, Hiroshi Y. Yoshikawa, Yuji Higaki, Atsushi Takahara, Takeshi Mori, Yoshiki Katayama, Akihiro Kishimura   +9 more
wiley   +1 more source

Identification and Discrimination of Sulfated and Unsulfated Gut‐Hormone Biomarkers in Human Serum by Nanopore

Small, EarlyView.
This study discriminates between sulfated and unsulfated cholecystokinin‐8 gut‐hormone forms at single‐molecule‐level resolution. Using an aerolysin nanopore embedded in a hybrid lipid‐polymer membrane, the system produces distinct electrical signatures enabling highly sensitive detection, even in 20% human serum.
Luca Iesu, Laurent Bacri, Juan Pelta, Benjamin Cressiot   +3 more
wiley   +1 more source

Interspecific Differences in the Effects on Embryos Between Freshwater and Marine Fish Exposed to Water‐Accommodated Fractions Derived From Very‐Low Sulfur Fuel Oil

Environmental Toxicology, EarlyView.
ABSTRACT This study evaluated the toxic effects of water‐accommodated fractions (WAFs) of very‐low sulfur fuel oil (VLSFO) on freshwater and marine fish embryos. Embryos of Japanese medaka (Oryzias latipes), Java medaka (Oryzias javanicus), and grass puffer (Takifugu alboplumbeus) were exposed to various concentrations of VLSFO‐WAF, and the effects on ...
Jumpei Matsuo, Shusaku Fukugami, Kei Nakayama, Masatoshi Yamasaki, Emiko Kokushi, Seiichi Uno   +5 more
wiley   +1 more source

Isotope Dilution NanoLC-MS/MS Quantitation of Methylglyoxal DNA-Protein Cross-Links: Formation and Repair in Human Cells. [PDF]

Anal Chem
Omondi RO, Barnes EM, Gurajala KC, Fisette G, Chaudray IA, Erber L.   +5 more
europepmc   +1 more source

Comparing the Effects of Microplastics From Conventional Cigarette Butts and Heated Tobacco Device: The Role of UV‐Induced Aging

Environmental Toxicology, EarlyView.
ABSTRACT Despite the widespread presence of cigarette butts in the environment, the potential toxicological effects posed by microplastics (MPs) derived from them remain poorly understood. In this study, we compared the effects of MPs from conventional cigarette butts (cellulose acetate) and heated tobacco devices (cellulose acetate and polylactic acid
Andraž Dolar, Veno Kononenko, Valentina Perc, Damjana Drobne, Gabriela Kalčíková, Jernej Imperl, Tina Skalar, Ula Rozman, Branka Mušič, Anita Jemec Kokalj   +9 more
wiley   +1 more source

Simultaneous quantification of cytidine, methylcytidine, and hydroxymethylcytidine by isotope-dilution LC-MS/MS with application to mouse liver samples. [PDF]

J Chromatogr A
Mishra P, Ma J, Xie H, Li F, Tsai RYL, Liang D.   +5 more
europepmc   +1 more source

Sugammadex interference with serum progesterone measurement: an in‐vitro study

Anaesthesia, EarlyView.
Summary Introduction Sugammadex may interfere with serum progesterone immunoassays, potentially rendering measured concentrations and resulting recommendations unreliable. Methods We investigated the effect of a range of sugammadex concentrations on serum progesterone concentrations in samples from pre‐menopausal female volunteers.
Tamblyn Devoy, Theresa Larkin, Miles Allan, Kevin Mantik, Monika McShane, Natalie A. Smith   +5 more
wiley   +1 more source