Results 111 to 120 of about 56,277 (295)

Aplicação da cromatografia gasosa bidimensional abrangente com microdetector de captura de elétrons para determinação de agrotóxicos em sedimentos

open access: yesQuímica Nova, 2011
Analysis of seven pesticides in sediments was successfully achieved using comprehensive two-dimensional gas chromatography with micro-electron capture detection, as it provided higher sensitivity and less matrix interference.
Juliana Macedo da Silva   +2 more
doaj   +1 more source

Protein‐Based High‐Performance Liquid Chromatography and Cyclodextrin‐Capillary Electrokinetic Chromatography for the Chiral Separation of Azoles

open access: yesELECTROPHORESIS, EarlyView.
Human serum albumin‐based high‐performance liquid chromatography and cyclodextrin‐based capillary electrokinetic chromatography were used for the chiral separation of azoles. Although only two of the five tested azoles could be enantioseparated by liquid chromatography, all of them were separated by capillary electrokinetic chromatography using single ...
Sarah Moreau   +3 more
wiley   +1 more source

Detection and Quantification Challenges in Microplastics Research: A Statistical Overview

open access: yesMicroplastics
Detection and quantification of microplastics are undermined by the absence of appropriate methods in some contexts—such as a statistically principled LOD for particle-count data—but more pervasively by the uncritical application of ostensibly simple ...
Fabio D’Ottaviano, Kyle Hart
doaj   +1 more source

Derivative spectrophotometric method for determination of acyclovir in polymeric nanoparticles

open access: yesQuímica Nova, 2012
A derivative spectrophotometric method was validated for quantification of acyclovir in poly (n-butylcyanoacrylate) (PBCA) nanoparticles. Specificity, linearity, precision, accuracy, recovery, detection (LOD) and quantification (LOQ) limits were ...
Guilherme Diniz Tavares   +6 more
doaj   +1 more source

By‐product of heparin extraction as a sustainable alternative to enhance the use of nitrogen in agriculture

open access: yesEnvironmental Progress &Sustainable Energy, EarlyView.
Abstract This study evaluates the potential of a new organic fertilizer derived from porcine intestinal mucosa (designated BHE), a by‐product of the heparin extraction process, as a sustainable nitrogen (N) source for agriculture. The work was conducted in two stages: (i) chemical and spectroscopic characterization of BHE compared with poultry litter ...
Aline Zanquetti   +3 more
wiley   +1 more source

Intentional Learning Theory: Validating Its Measurement

open access: yesSAGE Open
The purpose of this article is to describe and analyze the psychometric properties of the Learning Orientation Questionnaire (LOQ), which have not been previously published.
Sarah Mollman   +2 more
doaj   +1 more source

Extração de ácido trans-trans mucônico urinário com polímeros de impressão molecular e análise por cromatografia gasosa: espectrometria de massas

open access: yesQuímica Nova, 2012
This paper describes selective molecularly imprinted solid-phase extraction of ttMA from urine samples followed by derivatization and analysis by gas chromatography/mass spectrometry (GC/MS). The analytical calibration curve ranged from 0.3 to 7.0 mg L-1
Lidiane Silva Franqui   +3 more
doaj   +1 more source

Strategies for Identification and Mitigation of Sanguinarine in Mustard Oil Adulterated by Argemone—A Comprehensive Review

open access: yesFood Chemistry International, EarlyView.
Sanguinarine, a toxic alkaloid present in argemone, can lead to epidemic dropsy or chronic diseases through DNA intercalation and immune system suppression. Regulatory efforts face challenges due to economic motivations for adulteration as well as technical, social, and infrastructure barriers.
Gururaj Pejavara Narayana   +4 more
wiley   +1 more source

Determination of Aflatoxins and Selected Heavy Metals in Rice Varieties Cultivated in Fogera, Amhara Region, Ethiopia

open access: yesFood Chemistry International, EarlyView.
ABSTRACT Rice (Oryza sativa L.) is a vital staple crop for nearly half the world's population. This study investigates the levels of aflatoxins (AFB1, AFB2, AFG1, and AFG2) and selected heavy metals (Cd, Pb, and Cr) and essential elements (Mn, Fe, Mg, Cu, and Zn) in rice varieties cultivated in Fogera, Amhara Region, Ethiopia.
Melese Tilahun   +3 more
wiley   +1 more source

Q-LOQ: A Unified Approach to AI Fraud Detection and Post-Quantum Consumer Security

open access: yes
Presents Q-LOQ, a unified platform architecture addressing both the AI fraud crisis and the quantum security transition. Analyzes the convergent threat landscape of deepfake video, voice cloning, AI phishing, and synthetic identity fraud alongside the quantum computing threat.
Moosbrugger, Michael V.   +1 more
openaire   +3 more sources

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