Results 51 to 60 of about 124,083 (150)

A practical synthesis of the 13C/15N-labelled tripeptide N-formyl-Met-Leu-Phe, useful as a reference in solid-state NMR spectroscopy

Beilstein Journal of Organic Chemistry, 2008
A mild synthetic method for N-formyl-Met-Leu-Phe-OH (1) is described. After Fmoc solid phase peptide synthesis, on-bead formylation and HPLC purification, more than 30 mg of the fully 13C/15N-labelled tripeptide 1 could be isolated in a typical batch ...
Sven T. Breitung, Jakob J. Lopez, Gerd Dürner, Clemens Glaubitz, Michael W. Göbel, Marcel Suhartono   +5 more
doaj   +1 more source

Synthesis of Novel Arginine Building Blocks with Increased Lipophilicity Compatible with Solid-Phase Peptide Synthesis. [PDF]

Molecules, 2023
Glavaš M, Gitlin-Domagalska A, Ptaszyńska N, Starego D, Freza S, Dębowski D, Helbik-Maciejewska A, Łęgowska A, Gilon C, Rolka K.   +9 more
europepmc   +1 more source

Computer vision as a new paradigm for monitoring of solution and solid phase peptide synthesis. [PDF]

Chem Sci, 2023
Yan C, Fyfe C, Minty L, Barrington H, Jamieson C, Reid M.   +5 more
europepmc   +1 more source

Biradicals based on PROXYL containing building blocks for efficient dynamic nuclear polarization in biotolerant media

Journal of Magnetic Resonance Open
A versatile strategy for synthesizing tailored peptide based biradicals is presented. By labeling the protected amino acid hydroxyproline with PROXYL via the OH functionality and using this building block in solid phase peptide synthesis (SPPS), the ...
Kevin Herr, Mark V. Höfler, Henrike Heise, Fabien Aussenac, Felix Kornemann, David Rosenberger, Martin Brodrecht, Marcos de Oliveira, Jr., Gerd Buntkowsky, Torsten Gutmann   +9 more
doaj   +1 more source

Synthetic ramoplanin analogues are accessible by effective incorporation of arylglycines in solid-phase peptide synthesis. [PDF]

Chem Sci, 2023
Marschall E, Cass RW, Prasad KM, Swarbrick JD, McKay AI, Payne JAE, Cryle MJ, Tailhades J.   +7 more
europepmc   +1 more source

Mechanistic Study of Diketopiperazine Formation during Solid-Phase Peptide Synthesis of Tirzepatide. [PDF]

ACS Omega, 2022
Wang J, Berglund MR, Braden T, Embry MC, Johnson MD, Groskreutz SR, Sayyed FB, Tsukanov SV, White TD, Jalan A, Seibert KD, Kopach ME.   +11 more
europepmc   +1 more source

Label-Free Imaging of Solid-Phase Peptide Synthesis Products and Their Modifications Tethered in Microspots Using Time-of-Flight Secondary Ion Mass Spectrometry. [PDF]

Int J Mol Sci, 2023
Schmidt D, Maier J, Bernauer H, Nesterov-Mueller A.   +3 more
europepmc   +1 more source

Triethyl phosphate (TEP) as a green solvent for solid-phase peptide synthesis (SPPS)

Green Chemistry Letters and Reviews
Triethyl phosphate (TEP) is a new member of the Green Solid-Phase Peptide Synthesis (GSPPS) toolbox. TEP shows almost no toxicity and no carcinogenic or mutagenic properties. It degrades, giving the rather innocuous phosphoric acid and ethanol. TEP has a
K.P. Nandhini, Nosipho Cele, Beatriz G. de la Torre, Fernando Albericio   +3 more
doaj   +1 more source

Dipropylamine for 9-Fluorenylmethyloxycarbonyl (Fmoc) Deprotection with Reduced Aspartimide Formation in Solid-Phase Peptide Synthesis. [PDF]

ACS Omega, 2023
Personne H, Siriwardena TN, Javor S, Reymond JL.   +3 more
europepmc   +1 more source

Amino-Li-Resin-A Fiber Polyacrylamide Resin for Solid-Phase Peptide Synthesis. [PDF]

Polymers (Basel), 2022
Akintayo DC, de la Torre BG, Li Y, Albericio F.   +3 more
europepmc   +1 more source